I-chromatography ye-chromatography yensimbi yentsimbi yentsimbi

Inkcazo emfutshane:

I-capillary yinto ebaluleke kakhulu kwi-HPLC, edlala indima ebalulekileyo ekunxibelelaneni neemodyuli zesixhobo, kunye neekholamu zeChromatographic. I-Chrosir^®Iqela lifaka iikati ezintathu kunye nezixhobo ezinxulumene noko, ezenza ukuba zibe zii-capillaries ezintathu (uthotho lwe-Rulend, Ribend Series) ngeendlela ezahlukeneyo) ngeendlela ezahlukeneyo, kwaye zifumana amalungelo awodwa omenzi wechiza. Ungcelele lwe-capillary luhlolwe zii-SGS, luqinisekisa ngokupheleleyo izinto ze-capillary. I-capillary yeChroomar^®iyahambelana ne-95% ye-hplc.

Thumela i-imeyile kuthi

Iinkcukacha zemveliso

Iimpawu zeMveliso

Zintathu iintlobo ze-capillary yentsimbi engenasitayile: I-capillary ye-Run Comllary, Ribend Howillary kunye ne-Capline. Zonke i-capillary ithatha i-316l intsimbi engenanto njengezinto, nge-1.58mm (1 / i-1 / i-1 / i-1 / i-1 / 16inch i-Overlere kwiziphelo zombini, i-0.79mm (1inch) i-Opper engaphandle. Ukutsala umnxeba i-capillary yentsimbi engenasitayile idla ngokuba lilifa, kwaye lixhathise i-1200bar kunye ne-acid-bacala kakuhle. Zombini iziphelo ze-capillary yenzelwe ukuba ibe yindawo entle, ethintela ukuqhwaba. Iyabaphindisa i-1200bar kunye ne-acid-based kakuhle. Xa kuthelekiswa nothotho lwesalathiso, iRibend iname ixesha elide, kunye nengxaki enokuthi isetyenziswe kuphela kwintsimbi eqingqiweyo yesinyithi esifutshane. Zombini iziphelo ze-capline ye-Super Iyilelwe ngelungelo elilodwa lomenzi we "Drum"; I-capillary ilayishwe ngerhasi, emva kokuqiniswa komnwe, ukutywina kabini kweenqwelomoya kunye namacala anokufezekiswa. I-capillary idla ngokuba lilitye, elithintela ukwaphula. Ingayixhathisa ngaphezulu kwe-1200bar, kunye nesiseko se-acid. I-capillary kwaye ifanelekile ukuba yahlulwe kwaye ithathelwe indawo yedwa, kunye nobomi bamaxesha angama-150 (kwi-Compush yeKholakisi kunye nesixhobo). Xa kuthelekiswa ne-tranline kunye ne-Ribend Series, upapasho unokufumana ukusebenza kabini kokutywina, kufaka kuzo zonke iintlobo zekholam zeChromatographic, kwaye unciphise ivolumu enkeyikayo ye-capillary.

I-Stainis Steeces-Fobleillary yentsimbi ye-capillary ilula ukuyisebenzisa kwaye ikhawuleze ifake ngaphandle kwezixhobo, nangona isetyenziswa kwezona zixhobo ziphambili zeChilds kunye nokutshintsha ubumbeko lwe-chitromatographic kunye nokutshintsha ubumbeko lwe-chibsples. I-capillary efanelekileyo ihambelana neekholamu eziqhelekileyo zeCeromatographic kunye neeValves, kunye nokuxhathisa uxinzelelo lwenkqubo ukuya kuthi ga kwi-400 bar.

Iimbonakalo

I-1. Capillary yenziwa nge-316l tubing tub, ecocwe liqondo lobushushu.
2. Ukunganyangeki okuhle kwi-1200 bar kwaye ilungele uninzi lwezicelo.
I-3. Indawo egudileyo ngaphakathi kwetyhubhu yangaphakathi ukuze inciphise ukubuyela umva.
4. 1/16 i-intshi kuzo zombini iziphelo, ezifanelekileyo uninzi lwe-chromatograph ye-chromatograph.
I-5. Ukuqina komnwe okuqinileyo kuzo zombini izinto (ukumelana ne-400 bar), kufanelekile ukuba uninzi lwenkqubo ye-LC.
I-6. Iyafumaneka kwi-150mm / i-250mm / i-350mm / i-550mm ubude betyhubhu.
I-7. Ukuqina komnwe kukhululekile kukuhamba kwaye unokufaka isicelo kwi-chromatographs ezahlukeneyo.